abundance 10 0.4 0.3 0.2 0.7 0.6 0.8 1.0 0.9 271-s1_PROTON-1-2.jdf Quartet). 2.04 2.6 2.5 2.4 2.3 2.2 2.1 2.0 1.9 1.8 1.7 //\\\\ 2222 X: parts per Million : Proton 24A 1.6 1.5 1.4 1.3 3.06 (triplet) hex. 1.100 1.081 1.063 Filename Author Experiment Sample Id Solvent Actual Start Time Revision Time JEOL Data Format Dim Size X_Domain Dim_Title Dim_Units Dimensions Site Spectrometer Field Strength X_Acq Duration X_Domain X_Freq X_offset X_Points X Prescans X_Resolution X_Sweep 1.2 1.1 1.0 0.9 0.8 0.7 0.6 0.5 /|\ X_Sweep_Clipped Irr Domain Irr_Freq Irr_offset Tri_Domain Tri Freq Tri Offset Blanking clipped Scans Total_Scans Relaxation Delay Recvr Gain Temp Get = 271-a1_PROTON-1-2.j - byerep - proton.jxp <= 271-81 CHLOROFORM-D <= 15-NOV-2022 18:28:5 = 15-NOV-2022 17:55:2 = 1D COMPLEX <= 26214 <- Proton Proton = (ppm) X = Farmingdale State C - JNM-ECZ400S/L1 = 9.389766[T] (400 [ME -4.37256192 [a] - Proton = 399.78219838 [MHz] = 5(ppm) = 32768 <=0 = 0.22869888 [Hz] = 7.4940048 [kHz] = 5.99520384 [kHz] <= Proton = 399.78219838 [MHz] 5 [ppm] = Proton 399.78219838 [MHz] <- 5 (ppm) = 2[us] = FALSE =16 -16 <= 4 [s] 42 <= 18.1[dc] <= 6.067 [us] X 90 Width X_Acq Time X_Angle X Atn X_ Pulse Irr Mode Tri Mode Dante Loop Dante Presat Decimation_Rate Experiment Path Initial Wait Phase Presat Time Presat_Time_Flag Relaxation_Delay_Calc = 0[s] Relaxation_Delay_Temp = 4[s] Repetition Time -8.37256192 (a) = (0, 90, 270, 180 4[a] FALSE = 4.37256192 [s] = 45 [deg] = 1.3[dB] = 3.0335 [us] - Off - Off <=400 FALSE <= 0 = c:\Program Files = 1[a]

Introductory Chemistry: A Foundation
9th Edition
ISBN:9781337399425
Author:Steven S. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Donald J. DeCoste
Chapter15: Solutions
Section: Chapter Questions
Problem 10CR
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Please look at the Proton NMR spectrum and identify the proposed molecular structure. There is also a signal at 9.769 ppm indicating that an aldehyde is present 

abundance
0
0.2
0.1
0.3
0.4
2.6
0.5
0.6
0.7
0.8
1.0
0.9
271-s1_PROTON-1-2.jdf
2.04
(quartet).
2.5 2.4 2.3 2.2 2.1 2.0
//\\\\
X: parts per Million : Proton
1.9
1.8 1.7 1.6
1.5
24A
3.06
(triplet)
hex.
1.100
1.081
1.063
Filename.
Author
Experiment
Sample Id
Solvent
JEOLO
Actual_Start_Time
Revision Time
Data Format
Dim Size
X_Domain
Dim_Title
Dim Units
Dimensions
Site
Spectrometer
Field_Strength
X_Acq Duration
X_Domain
X_Freq
X_Offset
X Points
X_Prescans
X_Resolution
X_Sweep
1.4 1.3 1.2 1.1 1.0 0.9 0.8 0.7 0.6 0.5
/11
X Sweep_Clipped
Irr Domain
Irr_Freq
Irr Offset-
Tri Domain
Tri Freq
Tri Offset
Blanking
Clipped
Scans
Total_ Scans
Relaxation_Delay
Recvr_Gain
Temp Get
X 90 Width
= 271-s1_PROTON-1-2.j
byersp
= proton.jxp
= 271-81
= CHLOROFORM-D
= 15-NOV-2022 18:28:5
= 15-NOV-2022 17:55:2
X_Acq_Time
X_Angle
X Atn
X Pulse
Irr Mode
Tri Mode
Dante Loop
Dante Presat
Decimation Rate
Experiment Path
Initial_Wait
Phase
= 1D COMPLEX
= 26214
= Proton
= Proton
= (ppm]
= X
= Farmingdale State c
= JNM-ECZ400S/L1
= 9.389766[T] (400 [ME
= 4.37256192 [s]
= Proton
= 399.78219838 [MHz]
= 5(ppm)
= 32768
<= 0
= 0.22869888 [Hz].
= 7.4940048 [kHz)
= 5.99520384 [kHz]
= Proton
= 399.78219838 [MHz]
= 5(ppm]
= Proton
= 399.78219838 [MHz]
5 (ppm)
= 2 [us]
= FALSE
= 16
<= 16
= 4 [s]
= 42
= 18.1[dc]
= 6.067 [us]
= 4.37256192 [s]
45 [deg)
1.3[dB]
= 3.0335 [us]
= Off
= Off
= 400
= FALSE
= 0
= C:\Program Files\JE
= 1[s]
= (0, 90, 270, 180, 1
= 4 [s]
Presat_Time .
Presat_Time_Flag
= FALSE
Relaxation_Delay_Calc = 0[s]
Relaxation Delay_Temp = 4 [s]
Repetition Time
= 8.37256192[a]
Transcribed Image Text:abundance 0 0.2 0.1 0.3 0.4 2.6 0.5 0.6 0.7 0.8 1.0 0.9 271-s1_PROTON-1-2.jdf 2.04 (quartet). 2.5 2.4 2.3 2.2 2.1 2.0 //\\\\ X: parts per Million : Proton 1.9 1.8 1.7 1.6 1.5 24A 3.06 (triplet) hex. 1.100 1.081 1.063 Filename. Author Experiment Sample Id Solvent JEOLO Actual_Start_Time Revision Time Data Format Dim Size X_Domain Dim_Title Dim Units Dimensions Site Spectrometer Field_Strength X_Acq Duration X_Domain X_Freq X_Offset X Points X_Prescans X_Resolution X_Sweep 1.4 1.3 1.2 1.1 1.0 0.9 0.8 0.7 0.6 0.5 /11 X Sweep_Clipped Irr Domain Irr_Freq Irr Offset- Tri Domain Tri Freq Tri Offset Blanking Clipped Scans Total_ Scans Relaxation_Delay Recvr_Gain Temp Get X 90 Width = 271-s1_PROTON-1-2.j byersp = proton.jxp = 271-81 = CHLOROFORM-D = 15-NOV-2022 18:28:5 = 15-NOV-2022 17:55:2 X_Acq_Time X_Angle X Atn X Pulse Irr Mode Tri Mode Dante Loop Dante Presat Decimation Rate Experiment Path Initial_Wait Phase = 1D COMPLEX = 26214 = Proton = Proton = (ppm] = X = Farmingdale State c = JNM-ECZ400S/L1 = 9.389766[T] (400 [ME = 4.37256192 [s] = Proton = 399.78219838 [MHz] = 5(ppm) = 32768 <= 0 = 0.22869888 [Hz]. = 7.4940048 [kHz) = 5.99520384 [kHz] = Proton = 399.78219838 [MHz] = 5(ppm] = Proton = 399.78219838 [MHz] 5 (ppm) = 2 [us] = FALSE = 16 <= 16 = 4 [s] = 42 = 18.1[dc] = 6.067 [us] = 4.37256192 [s] 45 [deg) 1.3[dB] = 3.0335 [us] = Off = Off = 400 = FALSE = 0 = C:\Program Files\JE = 1[s] = (0, 90, 270, 180, 1 = 4 [s] Presat_Time . Presat_Time_Flag = FALSE Relaxation_Delay_Calc = 0[s] Relaxation Delay_Temp = 4 [s] Repetition Time = 8.37256192[a]
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