Consider a separation performed on a 30.0 mm long open tubular column with a 0.50 mm diameter and a 2.0 µm thick stationary phase. Compound A eluted at 12.63 min, compound B eluted at 13.24 min, and the unretained solvent eluted at 1.205 min. What are the adjusted retention times, t, and retention factors, k, for compounds A and B? TRA= TRB = 12.035 k = 9.5 KB = 10.0 11.425 What is the separation factor (relative retention), a, for this separation? Incorrect The widths at half-height, w₁/2, of the peaks for compounds A and B are 0.120 min and 0.253 min, respectively. Find the number of theoretical plates, N, and plate height, H, for each compound. NA = NB = HA= HB Incorrect Incorrect Incorrect Incorrect min min mm mm

Introduction to Chemical Engineering Thermodynamics
8th Edition
ISBN:9781259696527
Author:J.M. Smith Termodinamica en ingenieria quimica, Hendrick C Van Ness, Michael Abbott, Mark Swihart
Publisher:J.M. Smith Termodinamica en ingenieria quimica, Hendrick C Van Ness, Michael Abbott, Mark Swihart
Chapter1: Introduction
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Consider a separation performed on a 30.0 mm long open tubular column with a 0.50 mm diameter and a 2.0 µm thick
stationary phase. Compound A eluted at 12.63 min, compound B eluted at 13.24 min, and the unretained solvent eluted at
1.205 min.
What are the adjusted retention times, t, and retention factors, k, for compounds A and B?
TRA=
TRB = 12.035
k₁ = 9.5
KB = 10.0
What is the separation factor (relative retention), a, for this separation?
11.425
Incorrect
The widths at half-height, w₁/2, of the peaks for compounds A and B are 0.120 min and 0.253 min, respectively. Find the
number of theoretical plates, N, and plate height, H, for each compound.
NA =
NB =
HA=
HB =
Incorrect
Incorrect
Incorrect
Incorrect
The number of theoretical plates for the column is calculated as
N = √√N₁ × NB
X
Using N₁ and NB, calculate the expected resolution for this separation.
A
resolution:
Incorrect
min
min
mm
mm
Transcribed Image Text:Consider a separation performed on a 30.0 mm long open tubular column with a 0.50 mm diameter and a 2.0 µm thick stationary phase. Compound A eluted at 12.63 min, compound B eluted at 13.24 min, and the unretained solvent eluted at 1.205 min. What are the adjusted retention times, t, and retention factors, k, for compounds A and B? TRA= TRB = 12.035 k₁ = 9.5 KB = 10.0 What is the separation factor (relative retention), a, for this separation? 11.425 Incorrect The widths at half-height, w₁/2, of the peaks for compounds A and B are 0.120 min and 0.253 min, respectively. Find the number of theoretical plates, N, and plate height, H, for each compound. NA = NB = HA= HB = Incorrect Incorrect Incorrect Incorrect The number of theoretical plates for the column is calculated as N = √√N₁ × NB X Using N₁ and NB, calculate the expected resolution for this separation. A resolution: Incorrect min min mm mm
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